Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A
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Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. These tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as z262 corrosion, pitting, or stress-corrosion cracking.
ASTM A Intergranular Corrosion Testing and Analysis
This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens.
These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. Contact us now for pricing or a quote! Like what you saw? The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:.
Share on Tumblr Print. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in qstm oxidizing environments such as nitric acid. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type.
In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.
For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. The samples are weighed at each interval to determine mass asrm and degree of susceptibility to intergranular attack. How do you select the right ASTM corrosion testing method for your material?
Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: See Appendix X1 for information regarding test selection. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels.
A recent publication on intergranular corrosion.
A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and atsm not as effective for intergranular attack caused by other means.
Historical Version s – view previous versions of standard. The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. If materials with incorrect q262 treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to atsm.